The set-up is designed to demonstrate
and study the vapor-liquid equilibrium. As basic data of any
distillation problem is the equilibrium between the liquid and vapor
phases of the system subjected to distillation. Hence it is of great
importance to study the VLE.
The set-up consists of distillation still with a heating element, shell
& tube condenser, reflux & distillate section. A tank with pump
is provided to circulate cold water to condenser. Flow rates can be
regulated through control valve fitted. Instrumentation is done to
measure the temperatures at different points.
A Digital Temp. Controller is connected to heating element for precisely controlling & varying heat input. The vapors form the top of column are condensed in the shell and tube type condenser by circulating cooling water. The condensate is collected in reflux drum and feedback to column as reflux
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