The set-up is designed to demonstrate and study the vapor-liquid equilibrium. As basic data of any distillation problem is the equilibrium between the liquid and vapor phases of the system subjected to distillation. Hence it is of great importance to study the VLE.
The set-up consists of distillation still with a heating element, shell & tube condenser, reflux & distillate section. A tank with pump is provided to circulate cold water to condenser. Flow rates can be regulated through control valve fitted. Instrumentation is done to measure the temperatures at different points.
A Digital Temp. Controller is connected to heating element for precisely controlling & varying heat input. The vapors form the top of column are condensed in the shell and tube type condenser by circulating cooling water. The condensate is collected in reflux drum and feedback to column as refluxExperiments:
To determine the vapour Liquid Equilibrium curve for CCl4 and Toluene or any other mixtureFeatures:
Utilities Required:
Technical Details:
| Distillation still | MOC SS / Glass 1 Ltrs. Capacity. Insulated by ceramic wool & Nichrome wire Heating Mental |
| Condenser | Concentric Tube type |
| Cooling Water Tank | Material Stainless Steel, Capacity 20 litre |
| Water Circulation | FHP pump, Arrangement is done to vary & measure the flow rate. |
| Temp. Measurement | RTD PT-100 type Temp. Sensor |
| Control panel
|
Digital Temp. Controller 0-199.9°C for Distillation still, Digital Temp. Indicator: 0-199.9°C, with multi channel switch, On/off switch, Mains Indicator etc. |
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